Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide

P. V. Savitskii, R. I. Vas'Kevich, Yu L. Zborovskii, V. I. Staninets, S. A. But, A. N. Chernega

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Abstract

1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.

Original languageEnglish (US)
Pages (from-to)402-406
Number of pages5
JournalRussian Journal of Organic Chemistry
Volume44
Issue number3
StatePublished - Mar 2008

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ASJC Scopus subject areas

  • Organic Chemistry

Cite this

Savitskii, P. V., Vas'Kevich, R. I., Zborovskii, Y. L., Staninets, V. I., But, S. A., & Chernega, A. N. (2008). Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide. Russian Journal of Organic Chemistry, 44(3), 402-406.