1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.
|Original language||English (US)|
|Number of pages||5|
|Journal||Russian Journal of Organic Chemistry|
|State||Published - Mar 2008|
ASJC Scopus subject areas
- Organic Chemistry