Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide

P. V. Savitskii; R. I. Vas'Kevich; Yu L. Zborovskii; V. I. Staninets; S. A. But; A. N. Chernega

doi:10.1134/s1070428008030159

Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide

P. V. Savitskii
, R. I. Vas'Kevich
, Yu L. Zborovskii
, V. I. Staninets
, S. A. But
, A. N. Chernega

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.

Original language	English (US)
Pages (from-to)	402-406
Number of pages	5
Journal	Russian Journal of Organic Chemistry
Volume	44
Issue number	3
DOIs	https://doi.org/10.1134/s1070428008030159
State	Published - Mar 2008
Externally published	Yes

ASJC Scopus subject areas

Organic Chemistry

Access to Document

10.1134/s1070428008030159

Cite this

@article{65c43e98e42a4716818eedf5723567a3,

title = "Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide",

abstract = "1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.",

author = "Savitskii, \{P. V.\} and Vas'Kevich, \{R. I.\} and Zborovskii, \{Yu L.\} and Staninets, \{V. I.\} and But, \{S. A.\} and Chernega, \{A. N.\}",

year = "2008",

month = mar,

doi = "10.1134/s1070428008030159",

language = "English (US)",

volume = "44",

pages = "402--406",

journal = "Russian Journal of Organic Chemistry",

issn = "1070-4280",

publisher = "Pleiades Publishing",

number = "3",

}

TY - JOUR

T1 - Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide

AU - Savitskii, P. V.

AU - Vas'Kevich, R. I.

AU - Zborovskii, Yu L.

AU - Staninets, V. I.

AU - But, S. A.

AU - Chernega, A. N.

PY - 2008/3

Y1 - 2008/3

N2 - 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.

AB - 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide reacted with methyl iodide in the presence of sodium acetate in boiling ethanol to give 2,2′-dithiobis[N-(5-methylsulfanyl-4-phenyl-4H-1,2,4-triazol-3-yl) -benzenamine]. The reaction of the title compound with dimethyl acetylenedicarboxylate in dioxane led to the formation of methyl 3-(benzothiazol-2-yl)-2-(2-methoxy-2-oxoethyl)-2,3-dihydro-1,3, 4-thiadiazole-2-carboxylate.

UR - https://www.scopus.com/pages/publications/42449085713

UR - https://www.scopus.com/pages/publications/42449085713#tab=citedBy

U2 - 10.1134/s1070428008030159

DO - 10.1134/s1070428008030159

M3 - Article

AN - SCOPUS:42449085713

SN - 1070-4280

VL - 44

SP - 402

EP - 406

JO - Russian Journal of Organic Chemistry

JF - Russian Journal of Organic Chemistry

IS - 3

ER -

Heterocyclizations of 1-(Benzothiazol-2-yl)-4-phenylthiosemicarbazide

Abstract

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this