N,N′-dichloro-p-nitrobenzenesulfonamide (dichloramine-N) as a new oxidimetric reagent: Synthesis and analytical application

Netkal M. Made Gowda, V. M.Sadagopa Ramanujam, Norman M. Trieff, G. John Stanton, Dandinasivara S. Mahadevappa

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Abstract

A new oxidimetric reagent, dichloramine-N (N,N′-dichloro-p-nitrobenzenesulfonamide; DCN) has been synthesized and its structure elucidated from the spectral data and elemental analyses. The ultraviolet, infrared, nuclear magnetic resonance, and mass spectral data have been presented. Analytical applications of DCN as a potential redox titrant in the determination of diverse reductants such as ascorbic acid, methionine, sulfite, arsenite, glutathione, and indigocarmine have been described.

Original languageEnglish (US)
Pages (from-to)95-104
Number of pages10
JournalMicrochemical Journal
Volume26
Issue number1
DOIs
StatePublished - Mar 1981

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ASJC Scopus subject areas

  • Analytical Chemistry
  • Spectroscopy

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